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  1. Synthesis of a Biodegradable PLA: NMR Signal Deconvolution …

    Dec 16, 2021 · In this experiment, students performed a ring-opening polymerization (ROP) reaction in the laboratory and, then, collected a series of 1D NMR spectra with the aim of …

  2. NMR analysis and chemical shift calculations of poly (lactic acid ...

    Jun 13, 2012 · In this work, poly(lactic acid) (PLA) dimer model compounds with different tacticities were synthesized and studied in detail by 1H and 13C nuclear magnetic resonance …

  3. Dec 16, 2021 · In this experiment, students performed a ring-opening polymerization (ROP) reaction in the laboratory and, then, collected a series of 1D NMR spectra with the aim of …

  4. NMR Analysis of Poly(Lactic Acid) via Statistical Models - PMC

    The physical properties of poly(lactic acid) (PLA) are influenced by its stereoregularity and stereosequence distribution, and its polymer stereochemistry can be effectively studied by …

  5. NMR analysis and tacticity determination of poly(lactic acid) in …

    Sep 1, 2014 · A new analytical procedure is proposed in this work for the 1 H and 13 C NMR analysis of PLA. The procedure uses deuterated pyridine as the NMR solvent, which has been …

  6. In this work, poly(lactic acid) (PLA) dimer model compounds with different tacticities were synthesized and studied in detail by 1H and 13C nuclear magnetic resonance (NMR) in three …

  7. 1H NMR Spectroscopy in the Analysis and Characterization of Poly ...

    Sep 24, 2006 · High resolution 500 MHz 1 H NMR spectroscopy is a powerful tool for the analysis and characterization of poly(lactide) (PLA). It accurately provides information about the …

  8. mPEG-PLA and PLA-PEG-PLA nanoparticles as new carriers for …

    mPEG-PLA and PLA-PEG-PLA copolymeric nanoparticles with three different PLA to PEG ratios are synthesized and used for encapsulation of recombinant human Growth hormone (rhGH). …

  9. Synthesis of Polylactic Acid Oligomers for Broad-Spectrum ...

    The PLA oligomers were prepared by direct catalyst-free condensation polymerization of l-lactic acid monomers and characterized by FT-IR and 1 H-NMR. The antiviral results demonstrate …

  10. The Chemical Record - Wiley Online Library

    Jul 29, 2021 · NMR spectroscopy is a powerful analytical technique for the determination of the tacticity of PLA. This article describes in details the tacticity assignment for PLA derived from …

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